“分析测试技术论坛”——第11讲 ：核磁共振波谱仪（NMR）的理论和应用
讲座名称：
“分析测试技术论坛”——第11讲 ：核磁共振波谱仪（NMR）的理论和应用
讲座时间：
2018-10-25
讲座人：
Jonathan Iggo
形式：
校区：
兴庆校区
实践学分：
讲座内容：
讲座题目： Advanced Spectroscopic Elucidation for Chemists
讲座时间：2018年10月25日-27日
讲座地点：分析测试共享中心北109教室
讲座人：Jonathan Iggo 教授
讲座摘要：
This short lecture and workshop course is intended for synthetic organic and organometallic chemists and will describe how to apply modern NMR methods to the characterization of compounds in solution. The emphasis will be on how to apply and run the experiments discussed. The lectures will introduce how to apply and interpret 1D and 2D techniques to establish connectivity in, and hence the structure of, molecules. The lectures will be followed by practical
workshops in which participants will be taught how to perform, process and interpret the results of these experiments.
日程安排：
25 Oct.
9:00-11:10
Lectures on NMR
Quick review of basics
NMR spin; energy levels;
Chemical shift: referencing
Coupling: homo and heteronuclear coupling; decoupling
Multipulse NMR
1D; 2D basic structure of sequence
Connectivity
1D sequence
JMOD=APT
14:00-16:10
NMR workshop
26 Oct.
9:00-11:10
Lectures on NMR
selection of sequence
2D sequences
COSY and variants
TOCSY
HSQC, HMQC, HMBC (INADEQUATE, ADEQUATE)
Sensitivity
INEPT
DEPT and variants
HMQC
(HETCOR, obsolete)
14:00-16:10
NMR workshop
27 Oct.
Whole day event
NMR workshop
Conformation
nOe
NOESY 1D and 2D variants
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