“分析测试技术论坛”——第11讲 :核磁共振波谱仪(NMR)的理论和应用

讲座名称: “分析测试技术论坛”——第11讲 :核磁共振波谱仪(NMR)的理论和应用
讲座时间 2018-10-25
讲座地点 分析测试共享中心北109教室
讲座人 Jonathan Iggo
讲座内容

讲座题目: Advanced Spectroscopic Elucidation for Chemists
讲座时间:2018年10月25日-27日
讲座地点:分析测试共享中心北109教室
讲座人:Jonathan Iggo 教授
讲座摘要:
This short lecture and workshop course is intended for synthetic organic and organometallic chemists and will describe how to apply modern NMR methods to the characterization of compounds in solution. The emphasis will be on how to apply and run the experiments discussed. The lectures will introduce how to apply and interpret 1D and 2D techniques to establish connectivity in, and hence the structure of, molecules. The lectures will be followed by practical 
workshops in which participants will be taught how to perform, process and interpret the results of these experiments.

日程安排:

25 Oct.

9:00-11:10

Lectures on NMR

Quick review of basics

NMR spin; energy levels;

Chemical shift: referencing

Coupling: homo and heteronuclear coupling; decoupling

Multipulse NMR

1D; 2D basic structure of sequence

Connectivity

1D sequence

JMOD=APT

14:00-16:10

NMR workshop

26 Oct.

9:00-11:10

Lectures on NMR

selection of sequence

2D sequences

COSY and variants

TOCSY

HSQC, HMQC, HMBC (INADEQUATE, ADEQUATE)

Sensitivity

INEPT

DEPT and variants

HMQC

(HETCOR, obsolete)

14:00-16:10

NMR workshop

27 Oct.

Whole day event

NMR workshop

Conformation

nOe

NOESY 1D and 2D variants

 

 

 

讲座人介绍

Jonathan Iggo (JAI) is internationally recognized for his work in high resolution NMR studies of functional chemical systems, particularly his studies of organometallic catalysts mechanisms. He is regularly asked to contribute to has contribute review and “how to” articles on NMR, e.g. to The Encyclopaedia of Inorganic Chemistry and to Modern NMR Techniques for Synthetic Chemistry. He ran the NMR Service at the University of Liverpool for many years and is a member of the Management Committee of the RCUK Very-High Field NMR Facility for the Physical and Life Sciences located at the NMR Centre for Structural Biology at the University of Liverpool.

JAI has collaborated internationally with groups from Asia, the US, and Europe as well as other UK groups applying his unique NMR and HR-MAS instrumentation to the in situ identification of reaction intermediates and mechanisms and soft matter. His work on the mechanism of the Lucite ALPHA process was crucial to the successful commercialization of the process. His current research focuses on magnet resonance chemical shift imaging (CSI) of chemical and biological systems. 

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